TEM course – Bar-Ilan

Introduction to Transmission Electron Microscopy

Bar-Ilan University

Winter Semester, 2019

Sylabus

Transmission electron microscopy (TEM) is becoming more and more essential in many fields of research involving nano-scale structures.

The goal of this course is to provide the student with a basis upon which s/he can interpret electron microscopy results, understand the microscopy of others, and to know when (and when not) to turn to electron microscopy for answers concerning the microstructure of materials.

This course attempts to cover the basic topics required in all current microscopy techniques in use, and to delve into some of the more advanced techniques which are used in Materials Science.

The course is based on 14 lectures. In addition, the student is required to complete exercises which will be handed out during the course. A final exam will complete the course.

The final grade will be composed in the following manner:

  • 2 home exercises (50%)
  • 1 final exam (50%)

The lectures will be held on Wednesdays between 13:00-17:00 at the seminar room on the 9th floor of the Bar Ilan’s Institute for Nanotechnology and Advanced Materials (BINA).

Lecturer Details
Dr. Yaron Kauffmann
Phone #: 054-6563660
e-mail: mtyaron@technion.ac.il
Recommended Literature
* D.B. Williams and C.B. Carter “Transmission Electron Microscopy” Vol. 1-4, Plenum Press, New York (1996).
* D. Brandon and W.D. Kaplan, “Microstructural Characterization of Materials”, Wiley press, 2nd edition (2008).
* J.W. Edington, “Practical Electron Microscopy in Materials Engineering” (1976).
* J.C.H. Spence, “High-Resolution Electron Microscopy”, Oxford press, 3d edition (2003).
* R.F. Egerton, “Electron Energy-Loss Spectroscopy in the Electron Microscope”, Springer press, 3d edition (2011).
* Eric Stach, “MSE 640 Transmission Electron Microscopy and Crystalline Imperfections”, http://nanohub.org/resources/4092.

* to obtain a passwd for the PDF files please contact me

#DateTopics (+ lectures slides in flash** - no password needed)Handouts*
1+206/11/2019Introduction / Historical overview / Types of TEMs / Electron sources / Electron optics / Lens aberrations / Resolution / The vacuum system / Sample holders / Electron scattering in materials lectures 1 and 2 slides in flash
  • lectures #1-2
  • 3+420/11/2019Electron scattering in materials / Basic crystallography / Electron diffraction / The reciprocal space / Solving electron diffraction + JEMS / Laue zones lecture 3-4 slides in flash
  • lectures #3-4
  • JEMS SE WIN7
  • 5+604/12/2019Solving electron diffractions - exercises and practice / Dynamic diffraction / Kikuchi patterns / CBED / Contrast mechanisms - Mass-thickness / Diffraction contrast / Contrast from planar defects & interfaces lecture 5 slides in flash
  • lectures #5-6
  • 7+818/12/2019Contrast mechanisms - Diffraction contrast / Contrast from planar defects & interfaces / Phase contrast (HRTEM) - Fresnel Contrast / Moiré patterns / Lattice imaging / The CTF / Image delocalization / Cs correction lecture 7-8 slides in flash
  • lectures #7-8
  • Home Assignment #1 - submission date 08.01.20
  • HW #1
  • HW #1 solution
  • 9+1001/01/2020Quantitative analysis of phase contrast images / Phase contrast image simulations / Quantitative image processing & analysis / HRSTEM - BF/ADF/HAADF lectures 9-10 slides in flash
  • lectures #9-10
  • DM
  • 11+1215/01/2020Demo at the EM center / TEM Sample preparation lecture 12 slides in flash
  • lectures #11-12
  • Home Assignment #2 - submission date 06.02.20
  • HW #2
  • 13+1429/01/2020Analytical TEM - Electron energy loss spectroscopy (EELS) & EDS in the TEM / Pre-Exam Preparation lecture 12 slides in flash
  • lectures #13-14
  • Final exam - 16.02.20 / 12:30-14:30

    ** If you have problems playing the flash files please download it to your computer and use the STAND-ALONE FLASH PLAYER AVAILABLE HERE.

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