course 318525

Transmission Electron Microscopy in Materials Science

Technion Graduate Course #318525

Spring Semester, 2022

Room 401, Meidan building

Sylabus

Transmission electron microscopy (TEM) is becoming more and more essential in many fields of research involving nano-scale structures.

The goal of this course is to provide the student with a basis upon which s/he can interpret electron microscopy results, understand the microscopy of others, and to know when (and when not) to turn to electron microscopy for answers concerning the microstructure of materials.

This course attempts to cover the basic topics required in all current microscopy techniques in use, and to delve into some of the more advanced techniques which are used in Materials Science.

The course is based on 13 lectures. In addition, the student is required to complete exercises which will be handed out during the course. A final exam will complete the course.

The final grade will be composed in the following manner:

  • 2 home exercises (50%)
  • 1 final exam (50%)

The lectures will be held on Mondays between 12:30-14:20 at room 401 in the Maydan building (department of Materials Science & Engineering).

Lecturer Details
Dr. Yaron Kauffmann
Phone #: 4567
Office: Electron microscopy center (MIKA) office # EM12
e-mail: mtyaron@technion.ac.il
Recommended Literature
* D.B. Williams and C.B. Carter “Transmission Electron Microscopy” Vol. 1-4, Plenum Press, New York (1996).
* D. Brandon and W.D. Kaplan, “Microstructural Characterization of Materials”, Wiley press, 2nd edition (2008).
* J.W. Edington, “Practical Electron Microscopy in Materials Engineering” (1976).
* J.C.H. Spence, “High-Resolution Electron Microscopy”, Oxford press, 3d edition (2003).
* R.F. Egerton, “Electron Energy-Loss Spectroscopy in the Electron Microscope”, Springer press, 3d edition (2011).
* Eric Stach, “MSE 640 Transmission Electron Microscopy and Crystalline Imperfections”, http://nanohub.org/resources/4092.

* to obtain a passwd for the PDF files please contact me

#DateTopics (+ lectures slides in flash** - no password needed)2022 - Handouts*
121.03.22Introduction / Historical overview / Types of TEMs / Electron sources lecture 1 slides in flash
  • lecture #1
  • 228.03.22Electron optics / Lens aberrations / Resolution / The vacuum system / Sample holders lecture 1 slides in flash
  • lecture #2
  • 304.04.22Electron scattering in materials / Basic crystallography / Electron diffraction lecture 1 slides in flash
  • lecture #3
  • 411.04.22Electron diffraction & the reciprocal space / Solving electron diffractions - exercises and practice lecture 1 slides in flash
  • lecture #4
  • JEMS SE WIN7
  • 525.04.22Electron diffraction - Laue zones / Dynamic diffraction / Kikuchi patterns / CBED / Contrast mechanisms - Mass-thickness lecture 1 slides in flash
  • lecture #5
  • 609.05.22Contrast mechanisms - Diffraction contrast / Contrast from planar defects & interfaces / Phase contrast (HRTEM) - Fresnel Contrast lecture 1 slides in flash
  • lecture #6
  • 16.05.22No lecture - Workshop of the Annual meeting of the Israel Society of Microscopy (ISM)
    723.05.22Phase contrast (HRTEM) - Moiré patterns / Lattice imaging / The CTF / Image delocalization / Cs correction / Quantitative analysis of phase contrast images / Phase contrast image simulations lecture 1 slides in flash
  • lecture #7
  • Home Assignment - submission date 23.06.22
  • Home Assignment
  • Crystbox 64bit
  • 830.05.22Phase contrast (HRTEM) - Cs correction / Quantitative analysis of phase contrast images / Phase contrast image simulations / Quantitative image processing & analysis lecture 1 slides in flash
  • lecture #8
  • DM
  • 906.06.22Coherent & incoherent imaging / HRSTEM - BF/ADF/HAADF lecture 9 slides in flash
  • lecture #9
  • Dr. Probe Light
  • 1112.06.22Group #1 - Demo at the Titan / 08:30-10:30
    1013.06.22TEM Sample preparation lecture 10 slides in flash
  • lecture #10
  • 1115.06.22Group #2 - Demo at the Titan / 08:30-10:30
    1220.06.22Electron Energy Loss Spectroscopy (EELS) & Energy Filtered TEM (EFTEM) lecture 12 slides in flash
  • lecture #12
  • 1327.06.22Energy-dispersive X-ray spectroscopy (EDS) in the TEM / Advanced topics - Electron Tomography & iDPC / Pre-Exam Preparation lecture 123slides in flash
  • lecture #13
  • Energy table for EDS
  • Final exam - 14.7.22 / 10:00-12:00

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